Structural characteristics were determined using X-ray diffraction (XRD) analysis. The XRD analysis confirmed the presence of various phases of $ { {\rm TiO}_2}$ T i O 2 (anatase and rutile)...

Download scientific diagram | XRD pattern of SnO2 spheres with JCPDS of 41-1445 from publication: Synthesis of tin-glycerate and it conversion into SnO2 spheres for highly sensitive...

The observed XRD pattern confirms the formation of pure SnO2 polycrystalline phase, corresponding to a tetragonal crystal system with P42/mnm space group, and is found to be ...

X-ray diffraction (XRD) analysis indicates that the as-synthesized SnO 2 nanocrystallites consists merely of a rutile-type SnO 2 with tetragonal crystallographic structure. Scanning electron microscope (SEM) observation shows that the prepared SnO 2 nanoparticles are regularly rhombus in shape.

2022年11月1日 · In this work, the prepared TCO material SnO 2 has been characterized by XRD, UV–vis, Hall effect measurement, Thickness measurement, FESEM and EDX. From the XRD analysis we can conclude the crystallinity is increased after annealing. It is confirmed by the number of peaks observed after annealing and the improvement in the intensity of the peaks.

In the present work SnO2 nanoparticles were synthesized by two different methods using different precursors. In method 1 using SnCl4.5H2O a particle size of about 37nm was obtained and in method 2 using SnCl2.2H2O precursor, the size of the obtained nanoparticles were of the order of 9nm. XRD studies were conducted on the samples obtained by

XRD pattern reveals the formation of SnO 2 nanoparti-cles with polycrystalline phase demonstrating rutile structure [JCPDS Card No: 41-1445, a 4.743 Å. c 3.1859 Å]. The crystal planes (110), (101), (211), (002), (310), (301) were prominently seen in XRD indicat-ing the polycrystalline nature of powder. The average

2012年7月27日 · X-ray diffraction (XRD), field emission scanning electron microscopy, and transmission electron microscopy (TEM) were employed to characterize the as-prepared product, and optical property was studied by UV-visible diffuse reflectance spectroscopy (DRS).

2013年12月5日 · A range of diagnostic techniques including X-ray diffraction (XRD), UV–visible absorption, atomic force microscopy (AFM), scanning electron microscopy (SEM), and synchrotron-based X-ray photoelectron spectroscopy (XPS) were used to investigate structural, optical, and electronic properties of the resulting film.

2002年5月1日 · They found that a little deformation in the tin matrix of SnO 2 caused by the oxygen deficiency can induce the appearance of a layered structure, which is manifested by anisotropy in the XRD line widths, with the 101 line being the narrowest one. Also, the layered structure leads to the increase in crystallite sizes, and decrease in line ...